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They were merely used to produce the derivatives to generate the mass spectrometric information (full-scan spectra and SIM data) for evaluation. 33-m film thicknesses) interfaced to an Agilent 5975 mass selective detector (Palo Alto, CA). 0 mL/min). Injector, GCMS interface, and the ion source temperatures were set at 250, 290, and 230 oC, respectively. Various GC oven temperature and programming parameters were adapted for the analyses of the analytes and their ISs in various derivatization status or forms.

16% (contribution of SB to the intensity of the ion, m/z 268, designating SB-d5) used for theoretical calculation is too high. 4. Summary In essence, the evaluation of a set of CC data constitutes the following steps: (a) preparing sets of standard solutions ranging from low to high analyte concentrations; (b) comparing the empirically observed concentrations against the expected concentrations for each of these standard solutions, then plotting “the difference (in %) between these two values at each concentration” against “the concentration of the standard”; (c) calculating the concentrations that should theoretically be “observed” when the CC factor is taking into account, then plotting “the difference (in %) between this theoretically observed concentration and the prepared concentration” against “the concentration of the standard”; and (d) Comparing the plots obtained in steps “(b)” and “(c)” to assess the accuracy of the CC data used in calculating the “theoretically observed concentration” used in step “(c)”.

50. Willard HH, Merritt LL, Dean JA, Settle FA: Instrumental Methods of Analysis, 7th ed; Wadsworth Publishing: Belmont, CA; p. 32; 1988. 51. Krull I, Swartz M: Quantitation in method validation. LC•GC 16:1984; 1998. 52. Duncan MW, Gale PJ, Yergey AL: The Principles of Quantitative Mass Spectrometry; Rockpool Productions: Denver, CO; p. 97; 2006. Isotopically Labeled Analog as Internal Standard for Drug Quantitation — Methodology © 2010 by Taylor and Francis Group, LLC 31 PART TWO MASS SPECTRA OF COMMONLY ABUSED DRUGS AND THEIR ISOTOPICALLY LABELED ANALOGS IN VARIOUS DERIVATIZATION FORMS Figure I — Stimulants © 2010 by Taylor and Francis Group, LLC 33 Appendix One Mass Spectra of Commonly Abused Drugs and Their Isotopically Labeled Analogs in Various Derivatization Forms Table of Contents for Appendix One Figure I.

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A branch-reduce-cut algorithm for the global optimization of probabilistically constrained linear programs by Cheon M.


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